仿生UHMWPE关节软骨材料的静态黏弹性研究
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清华大学摩擦学国家重点实验室开放基金(SKLTKF08A01),江苏省自然科学基金(BK2008005)


Static viscoelastic properties of bionic UHMWPE articular cartilage material
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    摘要:

    目的 通过蠕变、应力松弛和蠕变回复等实验评价多孔梯度UHMWPE仿生软骨材料的静态黏弹性能。方法 采用模板滤取(T-L)法制备多孔梯度UHMWPE仿生软骨材料,扫描电镜观察多孔组织结构,压汞仪测量多孔层的孔隙率和孔径分布特征,平头压痕实验测定多孔梯度UHMWPE材料的蠕变、应力松弛和蠕变回复性能。结果 T-L法制备的UHMWPE梯度多孔层与基体的结合良好,随NaCl含量的增加,孔隙率增大,孔径尺寸分布范围扩大。蠕变变形和模量随时间呈非线性增加,应力松弛应力和模量非线性降低,对冲击载荷的缓冲能力明显高于致密UHMWPE。实验表明,具有合理孔隙率的U50和U60样品与致密UHMWPE材料回复性能相近,但过高的孔隙率造成蠕变回复的塑性变形增加。结论 多孔梯度结构UHMWPE材料的弹性增加,应变响应速度提高,有利于改善摩擦副的接触润滑状态,减轻材料的磨损。

    Abstract:

    Objective To evaluate the static viscoelastic properties of the porous gradient UHMWPE material by the creep, stress relaxation and creep recovery tests. Method The porous gradient UHMWPE material was prepared by the template leaching (T-L) method. The porous structure was characterized by scanning electron microscopy(SEM) and the porosity and pore distribution of porous layer were measured by a pressure mercury analyzer. The creep, stress relaxation and creep recovery properties were tested by the experimental determination of flat indentation. Results The porous layer of T-L UHMWPE was well bonded with the substrate material. With the increase of NaCl content, the porosity and pore size distribution scope improved clearly. Creep deformation and modulus presented a nonlinear increase with time and the stress and modulus of stress relaxation showed a nonlinear decrease with time. The buffering capacity for impact loads of porous gradient UHMWPE was significantly higher than the compact UHMWPE. Experimental results showed that the creep recovery properties of the reasonable porosity of U50 and U60 samples were almost similar to the compact UHMWPE material. But the higher porosity caused the increase of the plastic deformation. Conclusions The porous structure of UHMWPE effectively increased the elastic property and strain response sensitivity, which may be beneficial to improve the lubrication of frictional contact surfaces and reduce the wear of artificial joints.

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刘庆华,王庆良,沈涵,玄加申.仿生UHMWPE关节软骨材料的静态黏弹性研究[J].医用生物力学,2010,25(5):369-374

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  • 收稿日期:2010-08-25
  • 最后修改日期:2010-08-28
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